EFFECTS OF MOLE RATIO TO CHLORINE ADDED MAGNESIUM BORATE SYNTHESIS O AT 1000 C USING THE RAW MATERIALS OF MAGNESIUM CHLORIDE, MAGNESIUM OXIDE AND BORIC ACID
S. Piskin, S. E. Gurel, F. T. Senberber, A. S. Kipcak, E. M. Derun, N. Tugrul
Pages: 362-372
Published: 1 Jan 2013
Views: 464
Downloads: 54
Abstract: In today’s world, there are many application areas of boron and the studies about boron still continue. Boron is found in minerals with other elements in nature. Magnesium borates, which are a class of boron minerals, are the most important technical ceramics for their properties of; high heat-resisting, corrosion-resisting, super mechanical strength, superinsulation, light weight, high strength, and high coefficient of elasticity. In this study the solid-state method is applied to different stoichiometric mole ratios of MgCl2.6H2O, MgO and H3BO3. The characterization techniques of XRD, FT-IR and Raman are applied to the produced magnesium borates. From the XRD results three types of magnesium borates; boracite (Mg3B7O 13Cl), magnesium borate (MgB4O7) and suanite (Mg2(B2O5)), were formed. The highest crystalline minerals were obtained at the mole ratio of 1-6-14. Vibration analysis of FT-IR and Raman spectrums showed that the produced magnesium borates characteristic peaks were in good agreement with the literature.
Keywords: boric acid, magnesium borates, magnesium chloride, magnesium oxide, solid-state synthesis
Cite this article: S. Piskin, S. E. Gurel, F. T. Senberber, A. S. Kipcak, E. M. Derun, N. Tugrul. EFFECTS OF MOLE RATIO TO CHLORINE ADDED MAGNESIUM BORATE SYNTHESIS O AT 1000 C USING THE RAW MATERIALS OF MAGNESIUM CHLORIDE, MAGNESIUM OXIDE AND BORIC ACID. Journal of International Scientific Publications: Materials, Methods & Technologies 7, 362-372 (2013). https://www.scientific-publications.net/en/article/1003117/
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